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Original scientific paper

SUPERCRITICAL FLUID CO2 EXTRACTION ON LICHEN Usnea barbata L.

By
Kiril Lisichkov ,
Kiril Lisichkov
Contact Kiril Lisichkov

Faculty of Technology and Metallurgy, Saints Cyril and Methodius University of Skopje , Skopje , North Macedonia

Stefan Kuvendziev
Stefan Kuvendziev

Faculty of Technology and Metallurgy, Saints Cyril and Methodius University of Skopje , Skopje , North Macedonia

Abstract

Non-conventional separation procedure - supercritical fluid CO2 extraction (SFE-CO2) conforms to the strict demands of the precise process eco-technologies. It represents a perspective method especially in obtaining eco-friendly extracts from vegetable and animal raw materials. The influence of operating parameters (raw material’ granulation, extraction fluid’ flow rate, operating pressure, operating temperature and extraction time) on the yield of extract and usnic acid, has been studied throughout the extraction process on Usnea barbata L., by application of supercritical CO2 (SFE-CO2). The separation process in all experiments was conducted at operating temperature of 25 °C and operating pressure of 50-55 bar. The extraction of active components from the lichens by supercritical CO2 was performed in a highpressure, extraction “pilot-plant” for processing solid raw materials.

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Authors retain copyright. This work is made freely available online under an open-access model under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License (CC-http://creativecommons.org/licenses/by-nc-nd/4.0/BY-NC-ND 4.0).

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