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Original scientific paper

CHROMATOGRAPHIC BEHAVIOR AND LIPOPHILICITY OF N-(4-PHENYLSUBSTITUTED)-2,3-DIPHENYLPROPANAMIDES

By
Dj. Vaštag ,
Dj. Vaštag

Department of Chemistry, Biochemistry and Enviromental Protection, Faculty of Science, University of Novi Sad , Novi Sad , Serbia

N. Perišić - Janjić ,
N. Perišić - Janjić

Department of Chemistry, Biochemistry and Enviromental Protection, Faculty of Science, University of Novi Sad , Novi Sad , Serbia

S. Apostolov ,
S. Apostolov

Department of Chemistry, Biochemistry and Enviromental Protection, Faculty of Science, University of Novi Sad , Novi Sad , Serbia

S. Petrovic
S. Petrovic

Faculty of Technology and Metallurgy, University of Belgrade , Belgrade , Serbia

Abstract

Retention behavior of some N-(4-phenylsubstituted)-2,3-diphenylpropanamides was investigated on reversed phase thin layer chromatography (RP-C18). Retention constants of investigated compounds were determined in the following solvent systems: water-ethanol, watern-propanol and water-i-propanol. Linear relationships were obtained between retention, RM and volume fraction of organic solvent, ϕ. As a measure of lipophilicity of tested propanamides, Hansch`s lipophilicity parameter, π, were calculated. Chromatography retention constants RM0 were correlated with Hansch`s lipophilicity parameter, and good linear relationships were obtained. These results confirm, that retention constants, (RM0 ), determined in reversed phase thin-layer chromatography (RP-TCL) can be used, as criteria of lipophilicity.

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Authors retain copyright. This work is made freely available online under an open-access model under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License (CC-http://creativecommons.org/licenses/by-nc-nd/4.0/BY-NC-ND 4.0).

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