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Original scientific paper

SYNTHESIS AND STRUCTURAL ANALYSIS OF A Cu(II) COMPLEX WITH PYRIDOXAL S-METHYLISOTHIOSEMICARBAZONE (PLITSC) LIGAND

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Abstract

Reaction between a warm water mixture of pyridoxal hydrochloride (PL.HCl), and Smethyilisothiosemicarbazidehydroiodide (SMeTSC.HI) in the presence of Na2CO3 10 H O, we got pyridoxal S-methylisothiosemicarbazone (PLITSC; H2L). Ligand with appropriate Cu salt is coordinated, to give next complex: dark-brown, penta coordinated, square-pyramidal structure, mono(ligand)complex Cu(II) formula, [Cu(PLITSC)Br(CH3OH)]Br. In this work is given synthesis and structure of the complex with Schiff-based ligand.

Keywords: Pyridoxal-S-methylisothiosemicarbazone, Cu(II) complex, Synthesis, Crystal structure

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Published on
2010-12-31

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CC-BY-NC-ND 4.0