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Original scientific paper
Published: 31.12.2010.
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SYNTHESIS AND STRUCTURAL ANALYSIS OF A Cu(II) COMPLEX WITH PYRIDOXAL S-METHYLISOTHIOSEMICARBAZONE (PLITSC) LIGAND

By
S. Ivković ,
S. Ivković

Faculty of Environmental governance and corporate responsibility, Educons University , Sremska Mitrovica , Serbia

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V. Jevtović
V. Jevtović

Department of Chemistry, Faculty of Sciences, University of Novi Sad , Novi Sad , Serbia

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Abstract

Reaction between a warm water mixture of pyridoxal hydrochloride (PL.HCl), and Smethyilisothiosemicarbazidehydroiodide (SMeTSC.HI) in the presence of Na2CO3 .10 H O, we got pyridoxal S-methylisothiosemicarbazone (PLITSC; H2L). Ligand with appropriate Cu salt is coordinated, to give next complex: dark-brown, penta coordinated, square-pyramidal structure, mono(ligand)complex Cu(II) formula, [Cu(PLITSC)Br(CH3OH)]Br.In this work is given synthesis and structure of the complex with Schiff-based ligand.

Keywords:

Pyridoxal-S-methylisothiosemicarbazone,
Cu(II) complex,
Synthesis,
Crystal structure

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Authors retain copyright. This work is made freely available online under an open-access model under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License (CC-http://creativecommons.org/licenses/by-nc-nd/4.0/BY-NC-ND 4.0).

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Vol 2, Issue 2, 2010
SYNTHESIS AND STRUCTURAL ANALYSIS OF A Cu(II) COMPLEX WITH PYRIDOXAL S-METHYLISOTHIOSEMICARBAZONE (PLITSC) LIGAND PLANIRANJE LJUDSKIH RESURSA NA PRIMJERU METALOPRERAĐIVAČKOG PREDUZEĆA INFLUENCE OF APPLYING THE DIFFERENT ACIDS FOR ADJUSTING THE DYEBATH pH IN THE PROCESS OF DYEING THE POLYESTER KNITWEAR WITH DISPERSE YELLOW 3 FORMATION OF CARCINOGENIC SUBSTANCES DURING HEATING OF FOODS WHAT DETERMINES THE WATER QUALITY See full issue

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